Download e-book for iPad: Advances in Protein Chemistry, Vol. 5 by M.L. Anson, John T. Edsau (Eds.)

By M.L. Anson, John T. Edsau (Eds.)

ISBN-10: 0120342057

ISBN-13: 9780120342051

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Extra info for Advances in Protein Chemistry, Vol. 5

Sample text

183 (132) Bensoylglycyl chloride . . . . . . . . . . . . - (132) Beneoylglycylglycine . . . . . . . . . . . . 208 (132) Carbobenzoxyglycine. . . . . . . . . . . 120 (74) Carbobenzoxyglycyl chloride . . . . . . . . . 43 (74) Carbobenzoxyglycyl-a-aminoisobutyric acid . . . 164 (80) Carbobensoxyglycylglycine. . . . . . . . . . 178. (74) Carbobenroxyglycylglycinamide. . . . . . 179-181 (188) Carbobenzoxyglycylglycinhydrazide.

If monosubstitution products are sought, however, a different procedure must be employed. This special method depends on the fact that N-acylaspartic acid upon treatment with acetic anhydride gives an acid anhydride (cf. 67,203a). CHiCOOH - CHIC0 (CH8CO):O RCO-NH c: HCOOH In the case of the carbobenzoxy derivative, this reaction is not accompanied by racemization (74), unless sodium acetate also is present (186). The resulting carbobenzoxy-L-aspartic acid anhydride may be used for coupling reactions with alcohols to give monoesters and with amino acid esters to give carbobenzoxy-caspartyl peptide esters in which only one carboxyl group of aspartic acid is bound in peptide linkage.

123-124 (276s) .................. 136 (168) Chloroacetyl-cleucine. . . Toluenesulfonyl-Dbleucinhydrazide ........ 146 (266) Tolueneaultonyl-Dcleucylglycine.. ........ 5 (266) Toluenesulfonyl-calanyl-cleucine. 186 (266) Carbobenzoxyglycyl-cisoleucine. . . . . . . . . . Chloroacetyl-cisoleucine . . . . . . . . . . . . . 114-1 15 (277) 74-75 (16) be obtained in crystalline form by the procedure described by Bergmann and Zervas (74), although some workers have encountered difficulty in crystallizing this substance without inoculation with seed crystals.

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Advances in Protein Chemistry, Vol. 5 by M.L. Anson, John T. Edsau (Eds.)

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